Tetrahedron Letters (2020)
Update date:2022-08-05
Topics:
Palchykov, Vitalii A.
Gaponova, Rita G.
Omelchenko, Iryna V.
Kasyan, Liliya I.
A convenient method is reported for the multigram scale synthesis of compounds containing the novel octahydro-1H-2,5-epimino-4,7-methanoindene azapolycyclic system in good yields. This method involves the domino aminolysis of readily available dicyclopentadiene diepoxide in water at 165 °C. 2D NMR and XRD spectra of the products were studied in detail.
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