Journal of Organic Chemistry p. 775 - 778 (1981)
Update date:2022-08-02
Topics:
Hurley, Michael F.
Chambers, James Q.
Detailed procedures for the electrochemical reduction of carbon disulfide in N,N-dimethylformamide and acetonitrile are given.The synthetic utility of the method is demonstrated by the preparation of several thio-substituted derivatives of tetrathiafulvalene.Cyclic voltammograms of the tetrapotassium salt of the tetrathio anion of tetrathiofulvalene indicate four successive electron-transfer steps and in situ formation of a C6S8 species.Oxidation of the CS2 electrolysis solutions produces a compound which is tentatively identified as <1,3>dithiolo<4,5-d>-1,2,3-trithiole-5-thione.
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Doi:10.1007/BF00503664
(1981)Doi:10.1055/s-2004-829085
(2004)Doi:10.1021/ja01564a063
(1957)Doi:10.1016/0040-4020(80)80076-7
(1980)Doi:10.1139/v70-550
(1970)Doi:10.1055/s-1992-26273
(1992)
