Journal of the Chemical Society. Chemical communications p. 832 - 833 (1980)
Update date:2022-08-02
Topics:
Ambrosius, Huub P. M. M.
Noordik, Jan H.
Ariaans, Gerry J. A.
M(CO)3Cl(η5-C5H5) and M(CO)3(PPh3)2Cl2 (M = Mo, W) react with SPPh2H and Et3N to give M(CO)2(η5-C5H5)(η2-SPPh2) and M(CO)2(PPh3)(η2-SPPh2)2, respectively; an X-ray crystal structure determination of Mo(CO)2(PPh3)(SPPh2)2 reveals a 7-co-ordinate pseudopentagonal bipyramidal geometry for the molybdenum atom with an almost planar configuration for the sulphur and phosphorus atoms.
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