Journal of Organometallic Chemistry p. 233 - 242 (1992)
Update date:2022-08-04
Topics:
Couret, C.
Escudie, J.
Delpon-Lacaze, G.
Satge, J.
The metalation of chlorodiisopropylfluorenylsilane 1 with n-butyllithium leads to the α-silylthio compound 3.Compound 3 has a surprising stability and does not afford the diisopropyl(fluorenylidene)silene but behaves as its synthetic equivalent; i.e. it is a useful reagent for "Wittig-Peterson" reactions with various carbonyl compounds leading readily to diisopropylsilanone and fluorenylidene derivatives.
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