The Synthesis of Megaphone

DOI: 10.1021/ja00400a039

Source and publish data:

Journal of the American Chemical Society p. 2718 - 2721 (1981)

Update date:2022-08-02

Topics: Synthesis Characterization Yield Catalyst Nucleophilic substitution Purification Spectroscopy Reaction

Authors:

Buechi, George

Chu, Ping-Sun

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Article abstract of DOI:10.1021/ja00400a039

Condensation of 4,4,5-trimethoxy-2-<3-<(methylsulfonyl)oxy>propyl>-2,5-cyclohexadien-1-one (7) with 1,2,3-trimethoxy-5-(1-(Z)-propenyl)benzene in dichloromethane, in the presence of 1 equiv. of stannic chloride, gave (2β,3β,3aα)-3,3a-dihydro-5-methoxy-3-m

Full text of DOI:10.1021/ja00400a039

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Product name:(2β,3β,3aα,5β)-3,3a,4,5-tetrahydro-5-methoxy-3-methyl-3a-<3-<(methylsulfonyl)oxy>propyl>-2-(3,4,5-trimethoxyphenyl)-6(2H)-benzofuranone

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