Efficient electrochemical N-glycosylation of silylated pyrimidines with protected arylthioriboses in the presence of a catalytic amount of NBS or Br2

DOI: 10.1246/cl.1999.1053

Source and publish data:

Chemistry Letters p. 1053 - 1054 (1999)

Update date:2022-09-26

Topics:

Authors:

Nokami, Junzo

Osafune, Masahiro

Ito, Yuichiro

Miyake, Fumiaki

Sumida, Shin-Ichi

Torii, Sigeru

Read Full Text PDF DownLoad Join now for total 90,000,000 free articles

Article abstract of DOI:10.1246/cl.1999.1053

Electrolysis of silylated pyrimidines with protected arylthioribose, in the presence of a catalytic amount of NBS or Br₂ as a mediator in an undivided cell, gave the corresponding N-glycosides (nucleosides) in good yield.

Full text of DOI:10.1246/cl.1999.1053

Products guided by the article

Product name:1-(3,5-di-O-benzyl-2-deoxy-α-D-erythro-pentofuranosyl)thymine

Cas No:78138-03-1

R&D Labs maybe for 78138-03-1

Beijing Mediking Biopharm Co., Ltd.

Contact:+86-10-89753524/81760121/81769521

Address:Hongxianghong Incubator, Beiqijia Town, Changping district, Beijing, China
ZHANGJIAGANG FREE TRADE ZONE YONG HAN INTERNATIONAL TRADING CO., LTD(expird)

Contact:86 512 57910558

Address:qianjin M road
LIANYUNGANG YC FINE CHEMICAL CO., LTD

Contact:+86-518-858 99188

Address:Shangdong Modern Bldg, South Greenpark Road, Lianyungang, Jiangsu Pro. China
Haitong Chemical Industrial Co.,Ltd.

website:https://www.haitonglongwin.com/

Contact:+86-022-66221018

Address:18-701, No.99, The 4th Street, TEDA,
Chengdu Green Young Biopharmaceutical INC

Contact:+86-28-85337952

Address:1-B-26,Tianhe Industry Park, No.1480 of Tianfu Road,Chengdu,P.R.China,610000

Relevant to this article

Synthesis of [1,2,4]triazolo[1,5-a]pyrazines as adenosine A_2A receptor antagonists

Doi:10.1016/j.bmcl.2005.07.052
(2005)
Synthesis of N,N′,N″-trisubstituted thiourea derivatives and their antagonist effect on the vanilloid receptor

Doi:10.1016/S0960-894X(02)01040-5
(2003)
Extended mesoionic systems: Synthesis and characterization of monocyclic, polycyclic and macrocyclic pyrimidinium-olate derivatives and their photochemical behavior

Doi:10.1016/j.tet.2004.08.003
(2004)
Curtius rearrangement and Wolff homologation of functionalized peroxides

Doi:10.1016/j.tetlet.2004.08.059
(2004)
Chiral 1,4-Benzodiazepin-2-one, Template for Enantioselective Synthesis of α-Amino Acids and their α-Deuterio Congeners

Doi:10.1002/hlca.19810640420
(1981)
Alpha-(N-piperazino)dimethylacetanilides and their local anesthetic activity.

Doi:10.1021/jm00319a016
(1966)

Article Doi