Structural Modifications on Partially Silylated Carbohydrates by Means of Triphenylphosphane-Diethylazodicarboxylate, V (Transformations on Glyconolactones)

DOI: 10.1007/BF00911088

Source and publish data:

Monatshefte fur Chemie p. 215 - 240 (1981)

Update date:2022-07-29

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Authors:

Mark, Edgar

Zbiral, Erich

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Article abstract of DOI:10.1007/BF00911088

Reaction of D-glucono-1,5-lactone 1 with two equivalents of t-butyldimethylchlorosilane yields via a ring contraction 2,6-bis-O-(t-BDMSi)-D-glucono-1,4-lactone 2a as main product and a small amount of 5,6-bis-O-(t-BDMSi)-D-glucono-1,4-lactone 2c.Under the

Full text of DOI:10.1007/BF00911088

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