Bulletin of the Chemical Society of Japan p. 1711 - 1714 (1981)
Update date:2022-08-02
Topics:
Izumi, Takeo
Watabe, Hiroyuki
Kasahara, Akira
Reactions of 2-phenyl-4,4-dimethyl-2-oxazoline with lithium tetrachloropalladate(II) and palladium(II) acetate give dichlorobis(2-phenyl-4,4-dimethyl-2-oxazoline,3-N)palladium(II) and a cyclopalladated binuclear complex, di-μ-acetato-bis<2-(4',4'-dimethyl-2'-oxazolinyl)phenyl,1-C,3'-N>dipalladium(II), respectively.The latter complex is readily converted by a metathetical reaction with lithium chloride into its chloro-bridged analogue.The chloro-bridged complex reacts with triphenylphosphine to give the corresponding mononuclear ?-bonding palladium complex.All the complexes prepared in this study were characterized by means of IR and NMR spectroscopies.
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