2-Thiabicyclohepta-3,6-dienes. 3. Desulfuration and Sulfuration of 2-Thiabicyclohepta-3,6-dienes and X-ray Crystal Structure of 3a,6,7,8,9,9a-Hexahydro-3a,5-dimethylthienobenzothiophene-2,3-dicarbonitrile

DOI: 10.1021/jo00345a016

Source and publish data:

Journal of Organic Chemistry p. 977 - 982 (1982)

Update date:2022-08-04

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Authors:

Hall, Richard H.

Hertog, Herman, J. den

Reinhoudt, David N.

Harkema, Sybolt

Hummel, Gerrit J. van

Uiterwijk, Jos W. H. M.

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Article abstract of DOI:10.1021/jo00345a016

The-2-thiabicyclo<3.2.0>hepta-3,6-dienes 1-7 extrude sulfur in solution at 285 deg C to give the 1,2-benzenedicarbonitriles 8-12 in yileds of 42-56percent. 5-(1,1-Dimethylethyl)-3,6-dimethyl-2-thiabicyclo<3.2.0>hepta-3,6-diene-1,7-dicarbinitrile (6) react

Full text of DOI:10.1021/jo00345a016

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