Bulletin of the Chemical Society of Japan p. 208 - 211 (1982)
Update date:2022-08-05
Topics:
Inouye, Yoshinobu
Inomata, Satoru
Ishihara, Yasumasa
Kakisawa, Hiroshi
The Claisen rearrangement of 1-methyl-2-<(3-methylphenoxy)methyl>cyclopentene in N,N-dimethylformamide gave 5-methyl-2-(1-methyl-2-methylenecyclopentyl)phenol (5) via its trimethylsilyl ether. The methylation of 5, followed by a Simmons-Smith reaction and by the catalytic hydrogenolysis, afforded 3-hydroxycuparene.
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