Organic Magnetic Resonance p. 299 - 300 (1981)
Update date:2022-07-30
Topics:
Milosavljevic, Slobodan
Jeremic, Dragoslav
Mihailovic, Mihailo Lj.
Wehrli, Felix W.
Unambiguous signal assignments in the 13C spectra of monosubstituted cyclooctanones derived from the lead tetraacetate or silver oxide/bromine oxidations of the corresponding 1-monodeutero-alcohols have been obtained from deuterium-induced 13C isotope shifts and geminal and vicinal 13C-2H spin-spin coupling constants.The label in the ketones is shown to be in position 5.
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(1981)
