Tetrahedron Letters p. 2469 - 2472 (1999)
Update date:2022-07-30
Topics:
Bhat, Abhijit S.
Whetstone, Jennifer L.
Brueggemeier, Robert W.
A series of O-(t-butylsilyloxy)benzoyl chlorides generated from the corresponding silyl esters were coupled with a range of terminal alkynes to afford the corresponding alkynyl ketones. The alkynyl ketones were converted to enaminoketones and then cyclized to yield the desired benzopyrone ring system. This synthetic protocol utilizes readily available starting materials, mild and high yielding reactions with good functional group tolerance, and is ideal for developing combinatorial libraries centered around the benzopyrone ring system.
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