Journal of the Chemical Society. Chemical communications p. 364 - 365 (1988)
Update date:2022-08-04
Topics:
Jefford, Charles W.
Sledeski, Adam W.
Boukouvalas, John
Primary iodides alkylate 2-trimethylsiloxyfuran in the presence of a molar excess of silver trifluoroacetate to give the 4-alkylbut-2-en-4-olides in 55-81percent yield; as an illustration of the method, the cytotoxic marine sponge constituent, 4-(methoxycarbonylmethyl)but-2-en-4-olide was prepared in 79percent yield in one step.
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