Zeitschrift fur Anorganische und Allgemeine Chemie p. 1240 - 1242 (1999)
Update date:2022-07-30
Topics:
Baranov
Khvorykh
Troyanov
The reaction between PCl3 and ReCl5 yielded at 200 °C the ionic tetrachlorophosphonium dirhenium nonachloride, (PCl4)[Re2Cl9]. Single crystal X-ray diffraction analysis revealed a monoclinic unit cell: a = 8.616(3) A?, b = 10.449(4) A?, c = 9.397(3) A?, β= 99.72(3)°, V = 833.9(5) A?3, Z = 2, sp. gr. P21/m, wR2 = 0.1083 and R1 = 0.0527. The ionic compound is built from tetrahedra PCl4+ and face-sharing bioctahedra Re2Cl9-. The Re-Re distance, 2.724 A?, indicates the presence of direct Re-Re interaction.
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