Tetrahedron Letters p. 2155 - 2159 (2006)
Update date:2022-08-04
Topics:
Maraval, Valérie
Lepetit, Christine
Caminade, Anne-Marie
Majoral, Jean-Pierre
Chauvin, Remi
No catalyst pre-activation, no suicide alkyne, and no additive is required in an extremely simple procedure for the metathesis of alkyl-, alkenyl-, and aryl-propynes: just mix Mo(CO)6, p-chlorophenol, and the alkyne in 1,2-dichloroethane, heat at 85°C for 9-24 h, and the symmetrical alkyne is produced in ca. 95% yield.
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Doi:10.1016/j.tetlet.2006.01.117
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