Bulletin of the Chemical Society of Japan p. 611 - 612 (1984)
Update date:2022-07-29
Topics:
Harada
Sakakibara
Kunai
Sasaki
Several aromatic and aliphatic alpha , beta -unsaturated ketones were converted to the corresponding gamma -keto acids by the electrochemical reduction in acetonitrile in the presence of CO//2. The yields of the keto acid were 73-82% when the enones have at least one aromatic substituent. In the case of aliphatic enones, the yields of the carboxylation reaction were 67% for 2-cyclohexen-1-one and 44% for 3-buten-2-one.
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