Tetrahedron Asymmetry p. 1239 - 1248 (2000)
Update date:2022-08-03
Topics:
Tornoe, Christian W.
Sonke, Theo
Maes, Ilse
Schoemaker, Hans E.
Meldal, Morten
For the first time, enzymatic resolution of α-azido acid amides has been successfully demonstrated with high yields and enantiomeric excess. In one case dynamic kinetic resolution was achieved leading to more than 50% yield of the enantiomerically pure azido acid. Chiral HPLC was also used to separate racemic α-azido acids and the separation process was automated. Two routes to enantiopure α-azido acid building blocks for solid-phase peptide synthesis have, therefore, been established. Copyright (C) 2000 Elsevier Science Ltd.
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