Chemistry Letters p. 615 - 618 (1984)
Update date:2022-08-05
Topics:
Mukaiyama, Teruaki
Ohshima, Masahiro
Nagaoka, Hitoshi
Murakami, Masahiro
Alcohols are protected on treatment with 2-benzyloxy-3-fluoro-1-propene in the presence of a catalytic amount of PdCl2(COD), and the resulting acetals are easily deprotected to regenerate the parent alcohols by catalytic hydrogenation.The acetals, the protected alcohols, are rather resistant to acidic hydrolysis in comparison with common acetals because of the presence of fluoromethyl group.
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