
Carbohydrate Research p. 221 - 232 (1984)
Update date:2022-08-02
Topics:
Welch, John T.
Svahn, Britt-Marie
Eswarakrishnan, Seetha
Hutchinson, John P.
Zubieta, Jon
3-Acetamido-2,3,5,6-tetradeoxy-5-fluoro-D,L-ribo-hexofuranose was synthesized by direct, fluorinative dehydroxylation of methyl 3-acetamido-2,3,6-trideoxy-D,L-arabino-hexopyranoside with sulfur tetrafluoride-hydrogen fluoride.The furanose form and the ribo configuration, indicated by 13C- and 1H-n. m. r. spectroscopy, respectively, were confirmed by a single-crystal, X-ray diffraction study.
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