Journal of labelled compounds and radiopharmaceuticals p. 835 - 843 (1995)
Update date:2022-09-26
Topics:
Vermeulen
Sangaiah
Ball
Gold
2H and 13C-labelled bromodichloromethane and chlorodibromomethane were obtained in yields of 20 and 12% (for 2H) and 6 and 3% (for 13C) respectively from a convenient aluminum chloride-catalyzed reaction of bromoethane with commercially-available isotopically-substituted chloroform. The products were purified by preparative gas chromatography and-characterized by MS and 13C NMR, and by 1H for the 13C-labelled material; mass and nuclear magnetic resonance spectroscopy data are reported.
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