A new convenient synthesis of phosphoro(-no)chloridothionates

Article abstract of DOI:10.1080/00397919808004850

A general procedure for synthesis of phosphoro(-no)chlorides, particularly unsymmetrical ones, has been developed. The method involves the dealkylation of O,O-dialkyl phosphoro(-no)thionates 1 with dimethylamine and the chlorination of O-alkyl ammonium phosphoro(-no)thioates 2 using phosphorus oxychloride as a chlorinating agent.

Full text of DOI:10.1080/00397919808004850

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Synthetic Communications:
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Synthetic Organic Chemistry
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A New Convenient
Synthesis of Phosphoro(-
no)Chloridothionates
Zheng-Jie He a , Ju-Xiang Liu a & Chu-Chi Tang a
a State Key Laboratory of Elemento-Organic
Chemistry , Nankai University , Tianjin, 300071,
P.R. China
Published online: 20 Aug 2006.
To cite this article: Zheng-Jie He , Ju-Xiang Liu & Chu-Chi Tang (1998) A
New Convenient Synthesis of Phosphoro(-no)Chloridothionates, Synthetic
Communications: An International Journal for Rapid Communication of Synthetic
Organic Chemistry, 28:15, 2769-2772, DOI: 10.1080/00397919808004850
To link to this article: http://dx.doi.org/10.1080/00397919808004850
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