Journal of Organic Chemistry p. 2431 - 2435 (1985)
Update date:2022-07-29
Topics:
Clemens, Robert J.
Hyatt, John A.
The diketene/acetone adduct, 2,2,6-trimethyl-4H-1,3-dioxin-4-one, efficiently acetoacetylates aliphatic and aromatic alcohols, amines, and thiols.These acetoacetylation reactions are fast and stoichiometric, require no catalysis, and give only volatile byproducts.
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