Journal of the Chemical Society. Perkin transactions II p. 683 - 688 (1987)
Update date:2022-08-04
Topics:
Osman, Osman I.
McNaughton, Donald
Suffolk, Roger J.
Watts, John D.
Kroto, Harold W.
The conditions for and products of thermolysis of 4-azahepta-1,6-diyne, (HC<*>C-CH2)2NH, have been investigated by microwave, photoelectron, i.r., and mass spectrometric techniques.Prop-2-ynylideneamine, HC<*>C-CH=NH, is produced in good yield as well as penta-3,4-diene-1-yne, CH2=C=CH-C<*>CH, from (CH<*>C-CH2)2NH.Ionisation potential and vibrational data for HC<*>C-CH=NH, CH2=C=CH-C<*>CH, and the precursors have been obtained.The ionisation energies have been assigned with the aid of theoretical calculations.Photoelectron data on 3-aminopropyne, HC<*>CCH2NH2, have also been obtained.
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