Journal of Organic Chemistry p. 5179 - 5183 (1985)
Update date:2022-08-05
Topics:
Bartlett, Paul A.
Holm, Kjetil H.
Morimoto, Akira
A sequence utilizing selenolactonization of olefinic acid 4, Ireland-Claisen rearrangement of ketal ester 9, iodolactonization / epoxidation of olefinic acid 10, and regioselective hydrolysis of epoxide 15b is described for the stereocontrolled conversion of meso-2,4-dimethylglutaric anhydride to racemic tetrahydropyran lactone 1.
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