Convenient method for one-pot preparation of 1,2-diamines from nitroolefins

DOI: 10.1246/cl.1996.291

Source and publish data:

Chemistry Letters p. 291 - 292 (1996)

Update date:2022-07-29

Topics:

Authors:

Imagawa, Kiyomi

Hata, Eiichiro

Yamada, Tohru

Mukaiyama, Teruaki

Read Full Text PDF DownLoad Join now for total 90,000,000 free articles

Article abstract of DOI:10.1246/cl.1996.291

Convenient method for preparation of 1,2-diamine from the corresponding nitroolefin was established by successive reactions of Michael addition of O-ethylhydroxylamine to nitroolefin and reduction with hydrogen. The present preparative method was applicable to various nitroolefins by one-pot procedure.

Full text of DOI:10.1246/cl.1996.291

Products guided by the article

Product name:1-(4-methoxyphenyl)-ethylenediamine

Cas No:99250-51-8

R&D Labs maybe for 99250-51-8

Lanzhou huibang biological chemical technology Co., LTD

Contact:0931-7843964

Address:NO.2011,Yannan Road,Chengguan,
SHANXI XINTIANYUAN PHARMACEUTICAL CO., LTD.

website:http://www.tychemical.com

Contact:0086-358-3521713 3521715

Address:No. 1 Yintong Road, Shanxi Jiaocheng Economic Development Zone, Xiajiaying Town, Jiaocheng County, Lvliang City, Shanxi Province, China
Binzhou Holly Pharmaceutical Co.,Ltd.

Contact:74517

Address:No.15 Dapu Road,Huangpu District Shanghai,P.R.China
MINS GROUP CO.,LIMITED

Contact:18669908765

Address:Zibo City, Shandong Province, P.R.China
Hawks Chemical

Contact:+44 (0)161 367 9441

Address:

Relevant to this article

Catalyst-free synthesis of 3-sulfone nitrile from sulfonyl hydrazides and acrylonitrile in water

Doi:10.1039/c7ob01558e
(2017)
Synthesis of 14,15-dehydroerythromycin A ketolides: Effects of the 13-substituent on erythromycin tautomerism

Doi:10.7164/antibiotics.54.278
(2001)
The influence of phenolic hydroxy substitution on the electron transfer and anti-cancer properties of compounds based on the 2-ferrocenyl-1-phenyl-but-1- ene motif

Doi:10.1039/b705030e
(2007)
Synthesis of Carbocyclic Spiro Compounds from Isochroman Derivatives via Intramolecular Aldol Reaction

Doi:10.1055/s-1986-31849
(1986)
Cycloaddition of diphenylnitrilimine to coumarins. The synthesis of 3a,9b-dihydro-4-oxo-1h-benzopyrano [4,3-c]pyrazole derivatives

Doi:10.1016/S0040-4020(01)96550-0
(1985)
Syntheses of biologically important carbohydrates. 34. Syntheses of 3-C-methyl-branched hex-2-enopyranose derivatives and studies on the rearrangement of their trichloroacetimidates

Doi:10.1002/jlac.198619860402
(1986)

Article Doi