A Facile Synthesis of Aldehyde and Ketone via Sonochemical Barbier Reaction and Oxidation

DOI: 10.1002/jccs.199700010

Source and publish data:

Journal of the Chinese Chemical Society p. 65 - 69 (1997)

Update date:2022-08-16

Topics:

Authors:

Lee, Adam Shih-Yuan

Kung, Chih-Chun

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Article abstract of DOI:10.1002/jccs.199700010

Methyl ketone is prepared by a sonochemical Barbier reaction of methyl iodide, magnesium powder and aldehyde in Benzene/THF (9/1) solvent in a commercial ultrasonic cleaning bath (39 kHz), followed by the addition of N-chlorosuccinimide (NCS) as an oxidizing agent.

Full text of DOI:10.1002/jccs.199700010

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