The Journal of Organic Chemistry
Note
the sides of the NMR tube, before placing it under vacuum using a
rotary evaporator to remove all the remaining solvent. The tube was
then placed in a furnace and heated to 450 °C for 90 min (ramp rate =
10 °C min−1). The tube was then left overnight to cool slowly inside
the furnace to create a final robust, clear coating of anatase titania (ca.
1.4 mg cm−2, thickness ∼4 μm) on the inside of an otherwise
conventional Pyrex/quartz NMR tube (5 mm o.d., length = 20.3 cm).
XRD reveals the annealed TiO2 film is in its anatase crystal form.34
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AUTHOR INFORMATION
Corresponding Author
Notes
■
The authors declare no competing financial interest.
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