Tetrahedron Letters p. 687 - 690 (1997)
Update date:2022-08-16
Topics:
Gomez, Cecilia
Huerta, Fernando F.
Yus, Miguel
The reaction of 2-, 3- or 4-chlorobenzyl chlorides (1a-c) with an excess of lithium and a catalytic amount of DTBB (7 mol%) in the presence of different electrophiles [Pr(i)CHO, Bu(t)CHO, Et2CO, (CH2)5CO, PhCOMe, Me3SiCl] in THF at -50°C leads after hydrolysis with water, to the expected dioles or disilylated compounds 2aa-2cf.
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