Russian Chemical Bulletin p. 497 - 498 (1994)
Update date:2022-07-29
Topics:
Dodonov, V. A.
Gushchin, A. V.
Vorob'ev, O. G.
Zinov'eva, T. I.
Trimethylantimony(V) diacylates Me3Sb(OCOR)2 (R = H, Me, Ph) have been obtained in 72 - 75 percent yield by the interaction of trimethylantimony with tert-butylhydroperoxide and carboxylic acids at the ratio of 1:1:2 in benzene (20 deg C, 20 h) in the presence of sodium sulfate. - Key words: trimethylantimony(V) diacylates; synthesis, trimethylantimony; oxidative acylation.
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