Tetrahedron Letters p. 3413 - 3416 (1998)
Update date:2022-08-24
Topics:
Sugisaki, Claudia H.
Carroll, Patrick J.
Correia, Carlos Roque D.
The differential oxidation of five and six-membered endocyclic enecarbamates was investigated employing m-CPBA, DMD, as well as enantioselectivc protocols such as the Kochi-Jacobsen-Katsuki's epoxidation and the Sharpless dihydroxylation. By this strategy the syntheses of β- hydroxyprolines and β-hydroxypipecolic acids were accomplished, X-Ray crystallographic analysis of the trans-β-hydroxypipecolic acid was instrumental to solve structural assignment conflicts.
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