Tetrahedron Letters p. 8961 - 8964 (1994)
Update date:2022-08-11
Topics:
Soundararajan, Raman
Li, Guisheng
Brown, Herbert C.
2-Alkyn-1-ylboronates have been synthesized successfully, in excellent isomeric purity, via the in situ homologation of alkyn-1-ylboronates with LiCH2I. The relative reactivities exhibited by various LiCH2X reagents (X = Cl; Br; I) are described.
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