Zeitschrift fur Naturforschung, B: Chemical Sciences p. 426 - 429 (1998)
Update date:2022-08-11
Topics:
Minkwitz, Rolf
Schneider, Stefan
A preparation of trimethylsilanol by hydrolysis of bis(trimethylsilyl)carbonate in diethylether at -20 °C is reported. At -80 °C, the crystals are monoclinic, space group P21/c, Z = 12 with cell dimensions a = 996.0(2) pm, b = 1730.2(3) pm, c = 1122.9(2) pm, β = 96,61(3)°. There are three independent Me3SiOH units with a slightly distorted tetrahedral C3SiO core structure.
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