Tetrahedron p. 2949 - 2954 (1994)
Update date:2022-08-31
Topics:
Di Vona, Maria Luisa
Luchetti, Luciana
Rosnati, Vittorio
Ring cleavage was the main route in the Zn reduction of 1 in neat AcOH, while selective carbonyl reduction predominated in the presence of LiCl. The less strained 2 underwent only carbonyl reduction with Zn/AcOH. The Clemmensen reduction of both 1 and 2 resulted mainly in acyclic products. The unstrained 3 was fairly resistant towards reduction, and did not undergo ring cleavage.
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