Chemistry and Physics of Lipids p. 101 - 108 (1995)
Update date:2022-08-16
Topics:
Vieville, Corinne
Mouloungui, Zephirin
Gaset, Antoine
The C1-C18 alkyl oleates were prepared in n-hexane by esterification of oleic acid with either the primary and secondary C1-C6 alcohols or the primary fatty C8-C18 alcohols. The esterification was acid-catalyzed in the presence of p-toluene sulfonic acid (p-TSA) in a pseudo-homogeneous phase, or in the presence of the sulfonic macroporous resin (K2411) in the heterogeneous phase. The purified alkyl oleates were characterized by 13C-NMR. The oleic acid/alkyl oleate mixtures were analyzed by high-performance liquid chromatography (HPLC).
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Doi:10.1021/acs.bioconjchem.6b00461
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