Journal of the Chemical Society. Perkin transactions I p. 793 - 796 (1994)
Update date:2022-08-17
Topics:
Baker, Colin J.
Fray, Gordon I.
Geen, Graham R.
Ryan, Keith
Photocaging of the known Diels-Alder dimer of 2,3-dichlorocyclopentadienone, compound 1, followed by alkali-induced double ring-cleavage of the resulting caged diketone rac-2 or its dihydrate rac-3, led to the title tetrachloro dicarboxylic acid rac-5, thus affording a novel entry into the inherently chiral tricyclo<4.2.0.03,8>octane (C2-bissecocubane) system.Electrolysis of the disodium salt of rac-5- gave the tetrachloro alkene rac-14, from which other derivatives were obtained by standard methods.
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