Phosphorus, Sulfur and Silicon and the Related Elements p. 2385 - 2390 (2002)
Update date:2022-08-16
Topics:
Trofimov, Boris
Timokhin, Boris
Gusarova, Nina
Kazantseva, Marina
Golubin, Alexander
Oxidative phosphorylation of alkanols with white phosphorus in the presence of catalytic amounts of CuCl2 has been effected. The reaction proceeds in the aqueous H2O2-HCl system exothermically to form dialkylphosphites and trialkylphosphates in a total yield of up to 35%. Conditions for selective synthesis of dialkylphosphites in moderate yield have been found.
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