Collection of Czechoslovak Chemical Communications p. 2517 - 2522 (1993)
Update date:2022-07-30
Topics:
Mandel, Martin
Hudlicky, Tomas
Kwart, Lawrence D.
Controlled oxidation of chloroepoxide V with equivalents of sodium periodate furnished 2,3-O-isopropylidene-D-erythruronolactone (I) in 63percent yield.This procedure was augmented by combining the protection of diol III, the oxidation of acetonide IV to V, and the subsequent oxidative cleavage to I into one operation which yielded, on medium scale, the title lactone in 51percent yield.Detailed procedure of preparation and physical constants are provided for lactone I.
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