Bulletin of the Academy of Sciences of the USSR Division of Chemical Science p. 2599 - 2602 (1990)
Update date:2022-08-17
Topics:
Popkova, V. Ya.
Mysov, E. I.
Galakhov, M. V.
Osmanov, V. K.
German, L. S.
A new method has been developed for the synthesis of perfluorinated α,β-unsaturated thiocyanates by the reaction of the corresponding sulfenyl chlorides with KCN in water.The thiocyanate form of perfluoro-2-methyl-2-pentene-3-thiocyanate was isomerized to the isothiocyanate form.This rearrangement is initiated by both fluoride and thiocyanate anions.
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