Tetrahedron Letters p. 5299 - 5302 (1984)
Update date:2022-08-29
Topics:
Miyaji, Katsuaki
Nakamura, Toshio
Hirota,, Hiroshi
Igarashi, Michito
Takahashi, Takeyoshi
12β-Hydroxypicrasan-3-one, a compound having the correct relative stereochemistry of all the six ring-juncture chiral centers of the picrasane skeleton, was synthesized from a known tricyclic compound, using the orthoester Claisen rearrangement and lead tetraacetate oxidation as key reactions.
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