Journal of labelled compounds and radiopharmaceuticals p. 199 - 204 (1994)
Update date:2022-08-16
Topics:
Fielder
Rowan
6,6,6-2H3-2E-Hexenal, leaf-aldehyde, has been synthesised in 45% yield and 99.3% purity by reaction of 3,3,3-2H3-n-propyl magnesium bromide with an ethereal solution of 3-trimethylsiloxy-2-propenal (3) prepared in situ. This new one pot procedure alleviates the need to isolate (3) and should prove useful in the synthesis of other E-α,β-unsaturated aldehydes.
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