Russian Chemical Bulletin p. 1519 - 1525 (1999)
Update date:2022-08-10
Topics:
Ovcharenko
Fokin
Romanenko
Korobkov
Rey
Reduction of 2,3-dimethyl-2,3-dinitrobutane with Zn in aqueous ethanol in the presence of NH4Cl affords 2,3-bis(hydroxylamino)-2,3-dimethylbutane together with 2,3-diamino-2,3-dimethylbutane and complex Zn salts. A modified procedure was developed for the synthesis of bishydroxylamine, which involves reduction in a Zn/NH4Cl/THF-H2O system.
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