Tetrahedron Letters p. 2383 - 2385 (2006)
Update date:2022-08-29
Topics:
Titz, Alexander
Radic, Zorana
Schwardt, Oliver
Ernst, Beat
A safe and convenient method for the copper(II)-catalyzed diazo transfer from triflyl azide to primary amines is reported. By replacing CH2Cl2 by toluene the formation of hazardous side products, for example, azido-chloromethane and diazidomethane can be avoided.
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