Ring-Opening and Ring-Expansion Study of 3,4-Di(1-adamantyl)-1,2-dithiete

DOI: 10.1246/bcsj.71.1181

Source and publish data:

Bulletin of the Chemical Society of Japan p. 1181 - 1186 (1998)

Update date:2022-08-04

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Authors:

Nakayama, Juzo

Masui, Nobuo

Sugihara, Yoshiaki

Ishii, Akihiko

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Article abstract of DOI:10.1246/bcsj.71.1181

Reduction of 3,4-di(1-adamantyl)-1,2-dithiete (2) with LiEt₃BH, followed by treatment with Mel, gave (E)-1,2-di(1-adamantyl)-1,2-bis(methylthio)ethene (7-E) in 87% yield. Configuration of the double bond part of 7-E was determined by X-ray diff

Full text of DOI:10.1246/bcsj.71.1181

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