Tetrahedron Letters p. 6585 - 6588 (1997)
Update date:2022-08-24
Topics:
Hamann-Gaudinet, Beatrice
Namy, Jean-Louis
Kagan, Henri B.
Diiodosomarium prepared in THP reduces allylic iodides and bromides at 0 or -15°C to give organosamarium compounds which ore stable under these conditions. These allylic samarium compounds react with many functionalities including the keto group of keto esters. Benzylic samarium compounds were prepared similarly from benzylic bromides.
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