Chemistry Letters p. 721 - 724 (1980)
Update date:2022-08-17
Topics:
Matsumoto, Hideyuki
Ohkawa, Kazuhiro
Nakano, Taichi
Nagai, Yoichiro
In the presence of a catalytic amount of triphenylphosphine, 1,1,2,2-tetrachloro-1,2-dimethyldisilane reacted smoothly under mild conditions with carbon tetrachloride to produce (trichloromethyl)-methyldichlorosilane (1) in good yield. (Trichloromethyl)dimethyl-chlorosilane was also readily prepared by the triphenylphosphine-promoted transfer of the trichloromethyl group from (1) to dimethyldichlorosilane.
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