Journal of the Chemical Society, Dalton Transactions p. 1509 - 1512 (1982)
Update date:2022-08-16
Topics:
Lewis, Jack
Pardy, Richard B. A.
Raithby, Paul R.
Thermal decomposition of the known complex a = 9.072(4), b = 10.477(5), c = 13.921(7) Angstroem, α = 95.80(3), β = 93.54(3), γ = 102.48(3) degree, and Z = 2.The structure was solved by a combination of direct methods and Fourier-difference techniques and refined by blocked-cascade least squares to R = 0.039 for 3 084 diffractometer data.The Co(C5Me4Et) fragment caps the Os3 triangle.Each Os atom is also co-ordinated to three terminal carbonyl groups while the tenth carbonyl bridges an Os-Co bond.The complex
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