Tetrahedron Letters p. 5615 - 5616 (1998)
Update date:2022-08-29
Topics:
Malanga, Corrado
Mannucci, Serena
Lardicci, Luciano
The first one step synthesis of 2-methoxy-5-alkoxy-2,5-dihydrofurans (2a-i) is reported by reacting the commercially available 2,5-dimethoxy derivative (1) with alcohols. Unexpectedly the use of thiophenol and of cis- 2,4-but-2-enediol leads to 2-furyl phenyl thioether (4) and cis-2-propenal- 1,3-dioxep-5-ene (5), respectively.
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