
Journal of labelled compounds and radiopharmaceuticals p. 107 - 115 (1994)
Update date:2022-08-28
Topics:
Ekhato
Huang
A convenient method for the synthesis of phenylmethyl N-methyl[carboxy-14C]glycine hydrochloride (7) is described. It involves the carboxylation of transmetalated organostannane compound 4 which itself is accessible by established procedure. Success in preparing the labelled amino acid Z enabled us to synthesize target N-glycyl-N-methyl[carboxy-14C]glycine (10) by conventional coupling protocol.
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