Interactions in crystals. LXXIII. The structures of 1,2,4,5-tetrakis( trimethylsilyl) benzene and of its solvent-separated radical anion salt(H3COCH2CH2OCH3)3> >

DOI: 10.1016/0022-328X(95)00309-E

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Journal of Organometallic Chemistry p. 63 - 72 (1995)

Update date:2022-08-29

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Authors:

Bock, Hans

Ansari, Manssur

Nagel, Norbert

Havlas, Zdenek

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Article abstract of DOI:10.1016/0022-328X(95)00309-E

Reduction of 1,2,4,5-tetrakis(trimethylsilyl)benzene at a sodium-metal mirror under aprotic conditions and an argon atmosphere yields red needles of its solvent-separated radical anion salt.The structure, determined in a 150 K cold N2 flow, is discussed i

Full text of DOI:10.1016/0022-328X(95)00309-E

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