Synthesis of 2,6-dioxabicyclooctanes and 3,8-dioxabicyclodec-1(6)-enes by electrophilic cyclization of 3,4-dimethylene-1,6-hexanediols

DOI: 10.1007/BF00700900

Source and publish data:

Russian Chemical Bulletin p. 1262 - 1268 (1995)

Update date:2022-08-11

Topics:

Authors:

Gurskii, M. E.

Golovin, S. B.

Dekaprilevich, M. O.

Struchkov, Yu. T.

Bubnov, Yu. N.

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Article abstract of DOI:10.1007/BF00700900

3,4-Dimethylene-1,6-hexane diols 2 obtained by allylboration of ketones with 2,3-dimethylene-1,4-bis(dipropylboryl)butane 1 undergo cyclization on treatment with I2/NaHCO3 to give 1,5-cis-di(iodomethyl)-2,6-dioxabicyclo<3.3.0>octanes (4) and/or 3,8-dioxab

Full text of DOI:10.1007/BF00700900

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